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  • Dunder and Dragons: Making Rum at Lost Spirits Distillery

    Lost Spirits Distillery in Monterey County, California, is a kooky little place, resembling more a back yard miniature golf course than a typical distillery. Most of the equipment is outdoors, including the pot still that's shaped like a dragon, miniature grain-smoking pagoda, and the above-ground pool that serves as the cooling water for the condenser. 

    IMG_1469

    The distillery is run by Bryan Davis and Joanne Haruta. You may remember them from several years back when they ran a distillery in Spain that produced Obsello absinthe and Port of Barcelona gin. Davis is a former art teacher and zoo exhibit designer but he has picked up more than a little bit of chemistry as we'll soon see.

    So, that dragon-shaped pot still: It's powered by an old apartment building steam boiler for heat. The body of the still (300 gallons) looks like a big barbecue grill but it's made out of roofing copper. The shape was built in a way to minimize removing flavors, rather than rectifying much like tall round pot stills. Davis says, "We engineer the fermentation so much that we want to capture more of the flavor in distillation."

    IMG_1424
    IMG_1424

    The dragon tail is the lynne arm, which dips into a horizontal condenser. The water for the condenser comes from the bottom of a swimming pool, which heats up over the day of distilling, sometimes reaching 100 degrees Fahrenheit.

    With their old still, which was built out of wood, they would hop in the warm pool at the end of the day and use it as a hot tub. But chlorine and wood doesn't mix – the still actually got corked and they had to replace it. (For those of you barrel-aging cocktails, never rinse your barrels with chlorinated tap water for this reason.)

    Davis would like you to know that the pool water does not actually go into the whiskey; it stays in the pipes for cooling purposes only. 

    The dragon's head is a steam release, so while distilling steam shoots out its mouth. 

      IMG_1467
    IMG_1467

    Making Rum at Lost Spirits

    At this distillery they make whiskey and rum. The whiskey I wrote about for Whisky Advocate and I'll try to publish some more info here when the story comes out. 

    We watched an incredibly scientific Powerpoint presentation about the rum called, "Engineering Rum: The Fruit Nature Forgot to Make." I'll cover what I think I learned from it. 

    There will probably be some mistakes in the below text, so please don't take it as gospel but as starter info for further exploration. 

    • The goal, in part, as Lost Spirits, is to make high-ester rum 
    • A given rum may have up to 300 unique esters
    • Simple phenol smell is that familiar Band-Aid smell, but phenols as a group are a category
    • To make a high-ester rum, you need to make acids
    • Phenolic acids come from when we burn things. (In scotch whisky we're always talking about the phenol content of smoky whiskies.)
    • Lignin in sugar cane contains phenols you release by heating
    • For their rum, they want to start with a molasses that has high phenolics; has low anisoles (anise flavors); and is free of sulfur compounds. They use Grade-A molasses particularly for the latter reason. 

    Dunder

    • Rum nerds have heard about dunder pits- pits of decaying vegetation (and sometimes things like a rotting goat head) in wood-lined pits, found in old distilleries particularly on Jamaica. 
    • These pits acts as a bacteria starter. To these pits distillers in the olden days added stillage from distillation (the leftover stuff from distilling).
    • Then the dunder pit contents would be added to fermenting molasses to increase the esters in the rum distilled from it. 

    At Lost Spirits, they imitate the dunder pit process in a more… clean way. They mash up bananas and add lab-controlled bacteria to it. Then they add this to the fermenting molasses.  

    In the process of fermentation, there is a battle of yeast versus bacteria. The byproduct of yeast's battle against bacteria is acetic acid and trace carboxylic acid. Yeast under stress bind acids to alcohol and make esters. They accomplish this stress by adding dunder to yeast.

    As the goal is to get funky, stanky (high-esther, high-acid) rum out of the still, their still is a low-rectification model (short and squat). This will allow more of these compounds to pass over in distillation.  

    Aging Rum at Lost Spirits

    RumOne flavor they want to get out of their rum is a honey flavor, which is phenol-ethyl acetate. This comes from ethyl acetate (ester) plus phenol. And the ethyl acetate comes from from acetic acid (that comes from wood, yeast, and bacteria), wood as a catalyst, and ethanol. 

    Got that? Yeah me neither but sorta. 

    To age their rum they use new American oak barrels, smoked and charred to release lots more esters. These barrels are then seasoned with sherry. 

    Another flavor they want to crank up in their rum in rancio, a flavor found in old cognac and other spirits but that usually doesn't turn up until about 30 years of aging. However, Davis notes that it shows up earlier in solera-aged spirits, which are aged in super old barrels.

    Rancio comes from lignin (from long-aged wood barrels) decomposing in liquid. So they have figured out a way to copy this process and are patenting it. So all I know is what they're doing; not how. 

    Rums Coming Out of the Distillery

    Rums coming out of the distillery come in small batches and include Navy-style rum, Cuban-style rum, Colonial American-style rum, and Polynesian-style rum. I'm not sure what the difference is between the various styles, but they're all high-proof.

    I believe that the navy-style rum is the easiest to find. Some of it comes in at a whopping 68% and retails for about $45, which is an absurd bargain. 

    Science is delicious! 

     

  • Peru, Bird Poop, and the Birth of the Agro-Industrial Complex

    Last year while on a trip to Peru with Pisco Porton, we took a side trip to Las Islas Ballestas near the town of Paracas. The islands are important bird habitats, but more importantly they're covered in bird poop.

    Peru is an exciting country for drink nerds like me, as it is the birthplace of the potato, pisco, and the cinchona tree that produces quinine for tonic water. I didn't realize until recently that it was also the birthplace of the international guano industry, perhaps the world's first exported industrial fertilizer. 

    Guano, the bird poop that covers these ocean islands, is high in nitrogen, phosphate, and potassium, according to this surprisingly rich guano history page on Wikipedia. It is such a good fertilizer that it was exported to Europe in an era of Peruvian history from the 1840s to the 1870s called The Guano Age.

    (Much of the harvest of guano was performed by Chinese indentured servants, which is probably only interesting to me in that the same populations were dragged around the world to harvest sugar cane after slavery was abolished; another tie-in to the global booze business.)

    Recently, DNA testing has revealed that the Irish Potato Famine of 1845-52 may have been caused by new potato varieties imported along with Peruvian guano to Europe.

    And the end of international potato blight was the development of even more agro-chemicals, this time synthetic ones designed to cure the potato of the disease. 

    History is amazing.

    Here are some pictures from my visit to Las Islas Ballestas. 

    Ballestas Island Boat Tour Paracas Peru pelicans2
    Ballestas Island Boat Tour Paracas Peru pelicans2
    Ballestas Island Boat Tour Paracas Peru pelicans2
    Ballestas Island Boat Tour Paracas Peru pelicans2
    Ballestas Island Boat Tour Paracas Peru pelicans2
    Ballestas Island Boat Tour Paracas Peru pelicans2

     

  • Bars, Restaurants, and Sights of Lima, Peru

    In 2014 I visited Peru with Pisco Porton. In this post, I wanted to write up some places I visited in the city of Lima. I was only in town for about a day in a half, so I didn't see much. 

    Cocktail Bars and Restaurants in Lima

    Johnny Schuler's Key Club

    This restaurant is sort of like a speakeasy bar: It's open to the public, but there is no sign so you've gotta just know where it is. It looks very much like a place politicians and other power players would dine. I ate there with Schuler, who is the distiller of Porton. (He has a long history as a restaurateur and pisco television host before running his own distillery.) 

    Key Club Lima Peru Pisco Porton Tasting
    Key Club Lima Peru Pisco Porton Tasting

    amaZ

    This funky restaurant and bar in the Miraflores district specializes in fresh juices and herbs, with Amazonian ingredients in the food and drink and decor. There is a small central bar, lots of tables and chairs, and another dining room with wicker/rattan umbrellas over the top. 

    Amaz restaurant lima peru cocktail
    Amaz restaurant lima peru cocktail

    Malabar

    This restaurant has the same chef-owner as amaZ, but it's located in the San Isidro district. While it looked to be a ice restaurant, I sat at the bar and made friends with the bartender Jesus Avila Sovero. The restaurant is reportedly known for its Pisco Punch, which was sweet but nice. I also had a Chilcano (pisco and ginger ale) with anise; one with purple rice-infused pisco, tonic, and orange juice; and another with yellow tomatillo (that they call gooseberries). 

    This was definitely a good stop. 

    Malabar restaurant lima peru cocktails
    Malabar restaurant lima peru cocktails
    Malabar restaurant lima peru cocktails

    La Calesa

    The name means "buggy" or more likely "carriage" as you can see reflected in the hilarious laminated menu. Actually the whole place was pretty silly (located super close to Malabar) but I liked it. It is known for its traditional Pisco Sours, which are served double size.

    You can get those from a pre-batch or try any of the 16 pisco infusions featured on a shelf of jars. I had a Chilcano with camu-camu-infused pisco, as well as a touch of canela (cinnamon) pisco. I also tried the Algarrobina, which is sort of like eggnog but made with bean syrup. It was weirdly good. 

    La Calesa Restaurant Lima Peru Menu
    La Calesa Restaurant Lima Peru Menu
    La Calesa Restaurant Lima Peru Menu

    Huaca Pucllana

    This is a fancy/trendy restaurant adjacent to an ancient temple site from a civilization dating to 1000 years before the Incas. However it mostly looks like a pile of bricks. 

    The restaurant has a beautiful view though, over the ruins toward part of the city. 

    Huaca Pucllana temple Lima Peru7
    Huaca Pucllana temple Lima Peru7
    Huaca Pucllana temple Lima Peru7
    Huaca Pucllana temple Lima Peru7
     

     

     

  • Sights and Cities Along the Pisco Trail in Peru: La Ruta Del Pisco

    Last year I visited 5 distilleries in Peru with Pisco Porton (read about that visit here and here): Vinas de OroTres GeneracionesLovera, Hotel El Carmello, and La Caravedo where Porton is made.

    In other posts, I've written about the pisco distilleries that I visited along the pisco trail, aka La Ruta Del Pisco. This post is an overview of getting to the pisco region, where to stay, and things to see. 

    Coastal attractions along pisco trail Peru

    As you can see from the below maps, to tour pisco distilleries there is a long drive from Lima (the northernmost pin on the map) down the west coast of Peru to Ica, the southernmost cluster, passing the pisco producing towns of Chincha and Pisco. 

    In Ica we visited La Caravedo, the distillery that produces Pisco Porton. They were the host of my trip. 

    Peru world map
    Peru world map
    Peru world map

    Resources for Visiting the Pisco Region of Peru:

    • This page on the Peru Tourism website has information about distilleries. 
    • Here is a guidebook (PDF format) about visiting pisco distilleries in Ica. It's in Spanish but it has detailed information about distillery visits.
    • Should you want to arrange a tour or book a visit of the distilleries from Lima, Porton recommends using LimaTours or ContactTours.

    Sights along the Ruta Del Pisco

    El Piloto restaurant peruAs you can see, there are several pins on the map. The topmost is Lima, then the next pin along the ocean the Asia district. This is a seaside town and beach that seems mostly filled with local families. We stopped off for a great meal there at the modern restaurant El Piloto, but I'm not sure there is much else there to see for the international tourist. 

     

     

    Vinas de Oro Pisco Distillery Peru grapes 11The next two pins mark the city of Chincha and the distillery for Vinas de Oro. 

     

     

    Ballestas Island Boat Tour Paracas Peru seals3The next pin out in the water are the islands called Las Islas Ballestas, which are important for bird habitat and the production of guano.  

     

    Paracas street sceneThe district from which one takes a boat to Las Islas Ballestas is called Paracas. It is the most stylish of the towns we visited, with fancy hotels and it's where the wealthy residents of Lima come to relax. There are several large resort hotels, and it's probably the nicest place to stay if touring the pisco region of Ica, even though it's a big drive to Ica from there.

    Huacachina Oasis Peru10Ica is the city with lots of pisco distilleries, including La Caravedo (Porton), Bodega El Catador, and Hotel El Carmelo. On the outskirts of town is the oasis Huacachina. 

     

     

     

     

  • Distillery Visit: El Carmelo Distillery and Hotel in Ica, Peru

    Last year I visited 5 distilleries in Peru with Pisco Porton (read about that visit here and here): Vinas de Oro, Tres Generaciones, Lovera, Hotel El Carmello, and La Caravedo where Porton is made. This post is about my visit to El Carmelo in the region of Ica, Peru.

    El Carmelo is an unusual property, a quirky hotel and restaurant as well as a distillery. We only stopped in for dinner so I didn't learn much about it. The property's website is here

    It was dark so I didn't get great pics. Two are below. 

    El Carmello Peru hotel distillery restaurant2
    El Carmello Peru hotel distillery restaurant2

  • Distillery Visit: Lovera Pisco in Ica Peru

    Last year I visited 5 distilleries in Peru with Pisco Porton (read about that visit here and here): Vinas de OroTres GeneracionesLovera, Hotel El Carmello, and La Caravedo where Porton is made. This post is about my visit to Lovera in the region of Ica, Peru.

    Lovera is located in the village of Guadalupe in the region of Ica where there are around 120 distilleries. We were between places and decided to pop in on our way somewhere. 

    Lovera Distillery Pisco Peru sign3 Lovera Distillery Pisco Peru painting carrying botijas
    Lovera Distillery Pisco Peru painting carrying botijas

    This distillery is particularly rustic. Unlike most that have switched to stainless steel fermentation tanks, at Lovera they ferment in the traditional clay/ceramic botijas. Those are the tall containers you see located around distilleries. 

    Lovera Distillery Pisco Peru falca3
    Lovera Distillery Pisco Peru falca3
    Lovera Distillery Pisco Peru falca3
    Lovera Distillery Pisco Peru falca3
    Lovera Distillery Pisco Peru falca3

    We didn't really learn much about the production process here as we were just popping in, but we did stop in at the "bar," which was a single box under a canopy with a few chairs around it. 

    There were a couple of what I assume are the regulars. The guy on the right has a radio he is wearing around his neck. 

    Bar at Lovera Distillery Pisco Peru10
    Bar at Lovera Distillery Pisco Peru10

    Besides the pisco that they make there, we also had some of the local aperitif that they call "quita calzon" aka "panty remover." It is also called "perfecto amor" and in the US, the brand BarSol imports one. It is an aperitif drink; a combination of grape juice and pisco.

    In other countries, the similar aperitif (made from unfermented juice and the distilled product of that same juice) is called pineau des charantes (cognac), Floc de Gascogne (armagnac), and Pommeau (Calvados). 

    While at the bar, Porton's distiller Johnny Schuler told us the traditional way of drinking shots of pisco while sitting around in a group, as we were at this bar. One pours a shot into a shot glass, then pass the bottle to the next person. Then you take the shot and shake out the glass on the ground before passing the shot glass to the person with the bottle. Cheers. 

    Camper at Lovera Distillery Pisco Peru
     

     

  • Distillery Visit: Tres Generaciones Pisco in Ica, Peru

    Last year I visited 5 distilleries in Peru with Pisco Porton (read about that visit here and here): Vinas de OroTres GeneracionesLovera, Hotel El Carmello, and La Caravedo where Porton is made. This post is about my visit to Tres Generaciones in the region of Ica, Peru.

    Tres Generaciones is one of a few names you'll find used for this distillery tourist stop. The compound is called Tres Esquinas, and it also contains the restaurant La Olla de Juanita. 

    Bodega Dona Juanita Tres Generaciones Pisco Peru sign

    The distillery was founded in 1856. There is one distillery, but five families have the rights to use it. The distiller is Juanita Gonzalez. 

    The distillery has both types of stills used in pisco, the old-school falcas and the "modern" alembics that are the typical copper pot stills we usually see. 

    As mentioned in a previous post  about Pisco Porton's distillery La Caravedo, falcas are stills that are built as pits. The top part (at ground level) is a cap to open the still. It has no bubble shape on top like a traditional alembic, nor a lynne arm/swan's neck: It pretty much is a box with a tube near the top taking off the steam. 

    The steam is condensed in a typical copper coil, suspended in a big pool. 

    Bodega Dona Juanita Tres Generaciones Pisco Peru falca still

    The alembic stills look pretty standard, though they tend to be encased in brick (like cognac stills).

    Bodega Dona Juanita Tres Generaciones Pisco Peru still3

    We tasted a 60% ABV pisco right off the still, and it was soft, smooth, earthy, and grapey. Not citrusy at all and totally drinkable even at that proof. More than most spirits, pisco tastes delicious right off the still. I suppose it helps that by law it will never be watered down after its single distillation. 

    Below are a few more pictures from the distillery and restaurant.

    Bodega Dona Juanita Tres Generaciones Pisco Peru fermenting grape skins3
    Bodega Dona Juanita Tres Generaciones Pisco Peru fermenting grape skins3
    Bodega Dona Juanita Tres Generaciones Pisco Peru fermenting grape skins3
    Bodega Dona Juanita Tres Generaciones Pisco Peru fermenting grape skins3
    Bodega Dona Juanita Tres Generaciones Pisco Peru fermenting grape skins3
     

     

  • Distillery Visit: Pisco Vinas De Oro, Chincha, Peru

    Last year I visited 5 distilleries in Peru with Pisco Porton (read about that visit here and here): Vinas de OroTres GeneracionesLovera, Hotel El Carmello, and La Caravedo where Porton is made. This post is about my visit to Vinas de Oro in the region of Chincha, Peru.

    Chincha is a pisco-producing town south of Lima, on the way to Ica where all the other Peruvian distilleries I visited are located.

    Peru zoom3
     

    Vinas de Oro opened in 1983. According to Porton's distiller Johnny Schuler, Vinas De Oro's distiller began with a 5-liter still and now is in charge of this big operation of 8 alembic-style stills. (Older distilleries tend to have falca stills.)

    Vinas de Oro Pisco Distillery Peru entrance

    We visited the distillery near the end of the grape harvest. Workers were picking grapes off the vines in front of the distillery. According to the website, they grow, "seven types of Pisco grapes (aromatic: Italia, moscatel, torontel, albilla and non aromatic: quebranta, common black and mollar)."

    Vinas de Oro Pisco Distillery Peru vines4
    Vinas de Oro Pisco Distillery Peru vines4
    Vinas de Oro Pisco Distillery Peru vines4

    After the grapes are harvested, they are de-stemmed (to avoid tannins that would get magnified during distillation), then pressed with a bladder press to release the must (juice). The must is given a rough filtration.

    Vinas de Oro Pisco Distillery Peru grape skins2

    The juice is fermented for about 10 days (no yeast is added), so that it reaches around 10% ABV. The fermentation temperature is kept low (around 15 degrees Celsius) in order to retain aromatics from the grapes. 

    The wine is then distilled one time, as is the law. The pisco then rests for at least 10 months in stainless steel tanks. 

    Vinas de Oro Pisco Distillery Peru still5
    Vinas de Oro Pisco Distillery Peru still5

    The distillery bottles 6 puro piscos (individual grape varietals) and an acholado (blend). They also make mosto verde piscos, for which the grapes are not fully fermented before distillation to make the flavor fuller. They make mosto verde pisco out of three of their grape varietals. 

    The brand's website is here.

    Vinas de Oro Pisco Distillery Peru glass
     

     

  • Clear Ice Cubes Using a Tray in a Cooler

    Alcademics reader and ice nerd Mike Palmer has come up with an easy if not space-efficient way of making clear ice cubes using a silicone tray and a cooler.

    The short answer is: poke holes in the tray and set it on a riser at the bottom of an insulated cooler.

    The long answer? Palmer wrote it himself below.

     

    How to easily make perfect clear ice cubes, repeatably, from a tray

    By Mike Palmer

    Image.1.clear.ice.cube

    Here’s an easy way to make clear ice cubes in your freezer using an ice cube tray, obviating the need to carve individual cubes out of a block of clear ice.

    What you'll need: A small "Igloo" type cooler that fits in your freezer. A flexible, silicon ice cube tray with holes punched through the bottom. Something to make those holes, perhaps along with a piece of soft wood. A paper or Styrofoam cup. A rock. And of course, a freezer.

    Image.2.what.you.ned

    If TLTR, skip down to “How to do it.”

    Background

    I became obsessed with trying to make clear ice cubes at home (and later, clear ice spheres) after watching David Rees' How to Make an Ice Cube in his "Going Deep" series on the National Geographic TV channel. How hard could it be? (Ha!)

    BTW, after finally succeeding at making clear ice cubes, I found that there are tangible benefits from using them in your drinks. (Even if drinking water.) In addition to lasting longer (because they’re pure ice and not ice/air), clear ice cubes also taste better because they’re pure ice. That is, they don’t have yucky tasting freezer air in them. Also, women like the aesthetics of clear ice and they notice—and like—the sound clear ice cubes make clinking in a glass. (Sure to please.) Freezer cubes don’t clink. They clunk. And now you’ll notice every time you hear a sound track in a movie or on TV.

    In Theory

    In David Rees’ TV program, he showed how clear ice forms in nature when a body of water slowly freezes from the top down with a substantial mass of warmer, unfrozen water underneath. (Alcademics readers knew this back in 2009. See https://www.alcademics.com/2009/11/another-clue-to-ice-clarity-slow-freezing-like-a-japanese-pond.html.)

    And he suggested on his website that you could make a block of clear ice by kinda imitating nature, by letting a pan of water cool in a freezer. Although that’s not really imitating nature since the water in the tray freezes from the outside in on all sides.

    So freezing a pan of water does not make a clear block of ice, as even Mr. Rees concedes. Air still gets trapped in the middle, so you have to cut the “outer edges of your ice block” to harvest clear ice.

    Image.3.rees.screen.shot

    And even if the block were totally clear, you would still have to carve away at it to make individual cubes. And then you’d have to smooth six edges of each cube. that’s very time consuming, not to mention dangerous, working with sharp edged instruments on slippery ice.

    Rees’ suggestion for making clear ice works better if you use the slow freezing method, using a dorm style fridge set to 30 degrees, as Mr. Kevin Liu has suggested. https://sciencefare.org/2012/07/12/weird-science-ice-premium-ice-home/

    [note: the above link redirects to spam, try the Internet Archive version instead: https://web.archive.org/web/20150316061948/https://sciencefare.org/2012/07/12/weird-science-ice-premium-ice-home/]

    But you still get air in your cubes that way. Here’s a photo of an ice cube made that way. Air is still trapped in the last part of the cube to freeze. In this experiment, with only the center trays filled, that’s the bottom middle.

    Image.4.air.in.slow.freeze.tray

    (I hypothesize that air is sucked into the cube when the last bit of water expands as it freezes. It lifts the cube up and pulls a vacuum underneath. Interestingly, air gets trapped in different places in the different cubes depending on whether a cube has a sister cube (or cubes) next to it. You can tell what position in the tray the cube had come from based on the distribution of air trapped inside it. In one experiment, I filled the tray in a checkerboard fashion, so that no cube shared a side with another cube. Only their centers were cloudy.)

    In Practice

    What to do? I tried the slow freezing method, which was supposed to do the trick. But it didn’t.

    Fortunately we have the Internet. After searching around on youtube and seeing people consistently recommend “directional freezing,” I found Camper English’s Index of Ice Experiments on Alcademics. Camper was years ahead of everyone else.

    In Camper’s landmark experiment, he found that freezing water in molds in a cooler (that is, from the top down) gave clear ice.

    Image.5.campers.igloo.method

    Except that air got trapped in the very bottom of the ice.

    Image.6.air.in.campers.ice

    Why was that? Although Camper’s technique imitated the directional freezing aspect of nature, there was at least one other aspect missing: the large thermal mass of liquid water underneath the ice.

    So, building on Camper’s experiment, I placed a silicon ice cube tray on top of a large Styrofoam cup (as a stand) in a cooler. I filled the cup and I filled the cooler to the top of the ice cube tray. (That brought the water level halfway up the cooler. More on the optimal water level later.)

    I put the cooler in a high-end prosumer freezer, which was set at 0 degrees F, the government’s recommendation for food safety. (I checked the temperature in two places simultaneously using two digital thermometers in different locations in the freezer.)

    The result of this experiment was much better, but I still got a little bit of air trapped in the bottom of the cubes.

    Image.7.still.air.in.cube

    If you look at a close up Mr. Liu’s ice cube https://craftcocktailsathome.com/wp-content/uploads/2012/07/IMG_6874.jpg, his is not perfectly clear either.

    I hypothesized that there was still one more aspect of nature missing from this experiment, and that was that, unlike a Japanese ice pond, the water in the ice cube tray could not interact with the unfrozen water below it. One needed holes in the bottom of the ice cube tray for trapped air to escape.

    At the same time I came to this “Eureka!” moment, I found that a reader on the Alcademics blog had made the same observation. Furthermore, this idea was consistent with a suggestion on the blog of suspending a spherical ice ball mold upside down, above a pot of water, with the mold’s fill hole in the water to make a clear ice sphere. (Or similarly, the suggestion to put a spherical ice ball mold upside down (hole down) in a mug of water so that the water in the mold could interact with the unfrozen water below in the mug.)

    So here’s what I did.

    How to do it

    Image.8.acid.brush.8nd

    I took an acid brush and used the tube end as an auger to bore holes in the bottom of a silicon ice cube tray. Any similar tube will work. A 9mm shell casing would probably work too. (A .38 caliber casing is too large but works well on spherical ice molds.)

    I got my trays from Amazon, if you look closely at the photos of the ice cubes on the Amazon product page, you can see air trapped inside them.

    I used a Dremel tool with a cone-shaped cutter to grind a knife edge on the end of the tube. I put the ice cube tray on a piece of soft wood (to act as backing for the work) and pushed the tube into the bottom of the tray while rotating the tube. (If you use the end of an acid brush, you need to rotate it CCW so that the tube doesn’t unwind and open. If you use a shell casing, you can hammer on the casing (on the soft wood) to punch your holes through.)

    Image.9.auger.in

    Take a Styrofoam cup and cut it down to about an inch as a stand for the ice cube tray. (I started with a full size Styrofoam cup, but you’re just wasting water if you fill the cooler half full of water. And by using a one inch cup, the tray is lower in the cooler, resulting in better directional freezing.)

    Put’s a rock in the cup to weigh down the cup. Else, the stand floats off the bottom of the cooler.

    Image.10.rock.and.cup

    Put the tray in the cup that had the rock in it and filled the cooler with water to the top of the tray.

    Image.11.tray.in.water

    You might want to jiggle the tray a bit after you put it in the freezer, to knock air bubbles out that might be trapped underneath the tray.

    Wait about 18 hours. Timing is somewhat critical. You want to catch the freezing process just as ice has formed below the tray. If you wait too long, all the water below the tray will have frozen and you might get air in your cubes. Remember, in the Japanese pond, there is always unfrozen water below the clear ice.

    Image.12.its.done

    After the water under the tray has frozen, take the cooler out of the freezer, place it upside down in a sink and set a timer for about 10 to 20 minutes in case you forget to baby sit it. In about 10 or 20 minutes, you will hear a thunk as the ice block releases from inside the cooler. If you timed it right, a lot of water will eventually drain out of the cooler. (A cooler with the drain plug might be interesting. We could use compressed air to blow the ice block out.)

    You will be greeted by a strange formation of ice crystals and a cavern of sorts from where unfrozen water drained. (Apparently the cooler isn’t as well insulated on its bottom as we would like, since ice forms there. Since cold air descends, shouldn’t coolers be twice as thick on their bottoms as they are on their sides? Maybe we should put a cooler in a cooler?)

    Image.13.air.and.crystals

    Break the clumped ice away from the ice cube tray, push the cubes out of the tray from behind, and viola! Perfect, clear ice cubes.

    Allow your cubes to temper for one minute before using them in your drinks to avoid cracking. 

    Now you’re ready to do it all over again and make another batch!

    Image.14.viola

     

     

    High Strangeness

    When I first tried these experiments, I started with the minimal amount of water, not knowing what the right amount of water underneath the tray should be.

    I made a spacer that was only a half inch high.

    When I did that, something strange happened. I got an extrusion of cloudy ice during the freezing process!

    Image.15.extrusion

    It has always been a corner cube that extrudes in all my runs. All the other cubes are clear. That’s gotta be telling me something.

    So then I went the other way, putting more water in the mix by using a plastic beverage cup as a stand for the ice cube tray. I let the water freeze almost completely and didn’t get any extrusions. Let’s hear your thoughts about what’s causing the extrusions.

    Image.16.large.cup.stand

    You can see how the water has frozen at the bottom of the cooler, again demonstrating that the bottom of the cooler is not as insulated as it should be. In any event, there’s enough clear ice below the tray to give us clear ice cubes. (Notice some air bubbles just below the tray.)

    Ever being an engineer, I wondered what the “optimal” (minimal) amount of water was for this process. I kept shortening the cup until I got to one inch. Since I knew a half inch was too little, it seems that one inch is optimal. One inch seems to be about the same distance in the photo above too.

    I can now make perfect clear ice cubes repeatably in less than 24 hours without a lot of waste.

    —-

    Thanks Mike! 

    Read about all the ice experients on Alcademics by following this link. 

     

  • How Pisco Porton is Blended

    In 2014 I visited La Caravedo, the distillery where they make Pisco Porton. In this distillery there are really two distilleries, the old one dating to 1684 with primitive falca stills, and the shiny new one with copper pot/alembic stills.

    Read about the distillery set-up in the previous post

    Peruvian Pisco Law Review

    For Peruvian pisco (as opposed to Chilean – much Chilean pisco is column-distilled and and aged in wood), here are the laws of production:

    •  It must be made from one or more of 8 approved grape varietals. Aromatic grapes are Torontel, Italia, Albilla and Moscatel.  Nonaromatics are Quebranta, Negra Criolla, Uvina and Mollar.
    • These piscos made with the grapes can either be "puro," of all one variety; or "acholado," a blend of more than one.
    • They must be distilled a single-time in a falca or pot still.
    • Pisco must be distilled to a final proof of between 38 and 48 percent alcohol. Water is not allowed to be added to bring it down to final proof. 
    • It must be stored in nonreactive vessels (no wood barrels). 
    • "Mosto verde" pisco is made from grapes that are not fully fermented before distillation. This requires around 40 percent more grapes to produce. Mosto verde pisco can be made from any of the eight approved varietals or be a blend/acholado.

    Porton_Whitebackground_Hires

    Porton Actually Has 3 Sets of Stills

    1. Falcas, the old style stills at La Caravedo
    2. Pot/Alembic stills at La Caravedo
    3. Cognac-style pot stills at another of their vineyards

    This means that for any one grape varietal, they could make 3 different distillates as each still will produce a slightly different spirit. And they do. 

    How Porton Is Blended

    Pisco Porton is an acholado mosto verde, meaning it's a blend of mosto verde distillates. The 2014 bottling blend is:

    • Mosto Verde Quebranta distilled in falca stills at La Caravedo
    • Mosto Verde Quebranta distilled in alembic/pot stills at La Caravedo
    • Mosto Verde Quebranta distilled in cognac-style stills
    • Mosto Verde Italia distilled in cognac-style stills
    • Mosto Verde Abilla distilled in cognac-style stills
    • Mosto Verde Torontel distilled in  falca stills at La Caravedo

    The blend is:

    • 70% Quebranta
    • 1% Albilla
    • 25% Torontel
    • 4% Italia 

     Filtration:

    • After distillation, the spirit is rested. Then it is filtered before bottling.
    • First they chill the spirit to help precipitation naturally. No filter is used.
    • Then they use a cationic filter, which is a mix of resin and paper. This removes mineral and copper. (When we tasted un-blended piscos, a coppery note definitely showed through so it's clear this is needed.)

      La Caravedo Distillery Pisco Porton Peru tasting

     Component and Blend Tasting

    While at the distillery, I was able to taste several single grape varietals, in puro or mosto verde puro form. It was fascinating how different the varietals of grapes tasted from each other, and how different the same varietal could taste when put through a different still. 

    (Reminder, my tasting notes aren't supposed to make sense to other people.)

    • Mosto verde quebranta falca-distilled, freshly distilled: Hay, fresh-peeled banana, black olive tree. 
    • Mosto verde quebranta cognac still-distilled, rested 30 days: Similar but not as tasty
    • Blend of these two, married for 15 days: better than the sum of the parts
    • Mosto verde quebranta alembic-distilled, freshly distilled: headsy
    • Puro quebranta albembic-distilled 15 days ago (not mosto verde): Chex Mix, corn flakes, yeasty
    • Negra criolla (not sure which still or when distilled): Cantaloupe, wet wood finish
    • Albilla (not sure which still or when distilled): Fresh-picked blueberries, minerals, caramel
    • Moscatel mosto verde (not sure which still or when distilled): Dirt and violets. 
    • Italia column-distilled (so not pisco): Green tea mochi

    When I tasted the 2014 Pisco Porton blend, I could pick up so many of those individual grape varietal notes it all came together and I appreciate it so much more than I did in the past. It is complex with earthy minerals, musty, wet wood, deep structure, and grapey. I can't wait to taste it again.  

    La Caravedo Distillery Pisco Porton Peru old distillery5

     

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